Determinação de carbamato de etila em aguardentes de cana por CG-EM.

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2008
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A simple, specific and sensitive GC-MS procedure with ion m/z 62 was validated for the determination of ethyl carbamate (EC) in spirits. It exhibited linearity over the concentration of 30 to 600 μg/L with 30 μg/L limit of quantification. EC was detected in 70 of the 71 samples analyzed with levels from 33 to 2609 μg/L (mean level = 893 μg/L). 35% of the samples contained 500 to 1000 μg/L and 23% contained 150 to 500 and 1000 to 1500 μg/L. No significant correlation was found between EC and the levels of copper, pH and alcohol content of the samples.
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Sugar cane spirit, Ethyl carbamate
Citação
LABANCA, R. A.; GLÓRIA, M. B. A.; AFONSO, R. J. de C. F. Determinação de carbamato de etila em aguardentes de cana por CG-EM. Química Nova, v. 31, p. 1860-1864, 2008. Disponível em: <http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000700044>. Acesso em: 02 fev. 2015.